tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

Base Information

Chemical Name:tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate
CAS No.:1396514-87-6
Molecular Formula:C₁₈H₃₄BNO₄
Molecular Weight:339.283
Hs Code.:

Synonyms:tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

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Chemical Property of tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

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Technology Process of tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

There total 1 articles about tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 70557-99-2
2-(iodomethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 3712-40-1
tert-butyl cyclohexylcarbamate

: 1396514-87-6
tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

Guidance literature:: tert-butyl cyclohexylcarbamate; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 0.166667h;

2-(iodomethyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane; In tetrahydrofuran; hexane; at 20 ℃;
DOI:10.1021/ol301955s

Reference yield: 87.0%

: 1396514-87-6
tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

: 1397275-19-2
potassium tert-butyl cyclohexyl{(trifluoroborato)methyl}carbamate

Guidance literature:: With potassium hydrogen difluoride; In water; acetone; at 0 - 20 ℃; for 0.5h;
DOI:10.1021/ol301955s

Reference yield:

: 1396514-87-6
tert-butyl cyclohexyl{(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl}carbamate

: 1396518-01-6
tert-butyl cyclohexyl(4-methoxybenzyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydrogen difluoride / acetone; water / 0.5 h / 0 - 20 °C

2: chloro (2-dicyclohexylphosphino-2 ‘,4’,6’-triisopropyl-1,1’-biphenyl)[2-(2’-amino-1,1‘-biphenyl)]palladium(II); caesium carbonate / water; toluene / 3 h / 85 °C / Inert atmosphere

With potassium hydrogen difluoride; chloro (2-dicyclohexylphosphino-2 ‘,4’,6’-triisopropyl-1,1’-biphenyl)[2-(2’-amino-1,1‘-biphenyl)]palladium(II); caesium carbonate; In water; acetone; toluene; 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol301955s