3-Methoxybenzenesulfonamide

Base Information

Chemical Name:3-Methoxybenzenesulfonamide
CAS No.:58734-57-9
Molecular Formula:C7H9NO3S
Molecular Weight:187.219
Hs Code.:2935009090
European Community (EC) Number:640-249-8
DSSTox Substance ID:DTXSID10563752
Nikkaji Number:J409.572C
Wikidata:Q72489120
Mol file:58734-57-9.mol

Synonyms:3-Methoxybenzenesulfonamide;58734-57-9;3-methoxybenzene-1-sulfonamide;3-methoxybenzenesulphonamide;3-Sulphamoylanisole;benzenesulfonamide, 3-methoxy-;3-(Aminosulphonyl)anisole;m-methoxybenzolsulfonamid;m-Methoxybenzensulfonamid;SCHEMBL792467;DTXSID10563752;VBKIEQKVSHDVGH-UHFFFAOYSA-N;MFCD08704579;AKOS005254668;PS-4457;3-Methoxybenzenesulfonamide, AldrichCPR;CS-0252242;EN300-59542;Z234895027;(4S)-N-(TERT-BUTYLDIMETHYLSILYL)AZETIDIN-2-ONE-4-CARBOXYLICACID;G8F

Suppliers and Price of 3-Methoxybenzenesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
3-Methoxybenzenesulfonamide
100mg
$ 60.00

SynQuest Laboratories
3-Methoxybenzenesulfonamide
1 g
$ 120.00

SynQuest Laboratories
3-Methoxybenzenesulfonamide
5 g
$ 280.00

SynQuest Laboratories
3-Methoxybenzenesulfonamide
250 mg
$ 32.00

Matrix Scientific
3-Methoxybenzenesulfonamide 97%
1g
$ 31.00

Matrix Scientific
3-Methoxybenzenesulfonamide 97%
5g
$ 130.00

Crysdot
3-Methoxybenzenesulfonamide 95+%
100g
$ 743.00

Apolloscientific
3-Methoxybenzenesulphonamide
250mg
$ 29.00

Apolloscientific
3-Methoxybenzenesulphonamide
5g
$ 254.00

Apolloscientific
3-Methoxybenzenesulphonamide
1g
$ 109.00

Total 15 raw suppliers

Chemical Property of 3-Methoxybenzenesulfonamide

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Melting Point:131-133 °C
Refractive Index:1.553
Boiling Point:363.9 °Cat760mmHg
PKA:10.12±0.60(Predicted)
Flash Point:173.9 °C
PSA：77.77000
Density:1.314 g/cm³
LogP:2.12370
XLogP3:0.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:187.03031432
Heavy Atom Count:12
Complexity:232

Purity/Quality:

99% ^*data from raw suppliers

3-Methoxybenzenesulfonamide ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=CC=C1)S(=O)(=O)N

Technology Process of 3-Methoxybenzenesulfonamide

There total 5 articles about 3-Methoxybenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3-methoxybenzenediazonium tetrafluoroborate

: 58734-57-9
3-methoxybenzenesulfonamide

Guidance literature:: With sodium metabisulfite; sodium azide; tetrabutylammomium bromide; triphenylphosphine; In water; acetonitrile; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1039/c8gc03014f

Reference yield: 91.0%

: 10130-74-2
m-Methoxybenzenesulfonyl chloride

: 58734-57-9
3-methoxybenzenesulfonamide

Guidance literature:: With ammonium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; Inert atmosphere;

Reference yield:

: 766-85-8
3-methoxy-1-iodobenzene

: 58734-57-9
3-methoxybenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-diazabicyclo[2.2.2]octane-triethylenediamine-bis(sulfur dioxide); palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate / 1,4-dioxane / 16 h / 70 °C / Inert atmosphere

2: acetic acid; zinc / 25 °C / Inert atmosphere

3: acetic acid; zinc / 25 °C / Inert atmosphere

With 1,4-diazabicyclo[2.2.2]octane-triethylenediamine-bis(sulfur dioxide); palladium diacetate; acetic acid; tri tert-butylphosphoniumtetrafluoroborate; zinc; In 1,4-dioxane;
DOI:10.1039/c2ob07034k