Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol^(2-))

Base Information

• Chemical Name: Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol^(2-))
• CAS No.: 666826-42-2
• Molecular Formula: C₄₄H₄₂N₂O₇P₂Pd
• Molecular Weight: 879.194

Synonyms:Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol^(2-))

Chemical Property of Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol^(2-))

Chemical Property:

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Technology Process of Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol^(2-))

There total 1 articles about Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol^(2-)) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(1,2-ethanediylbis[bis[4-(1-methylethenyl)phenyl]-phosphine])PdCl2 + 4,6-dinitropyrogallol (3264-71-9) → Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol(2-)) (666826-42-2)

Guidance literature:

With KOH; In dichloromethane; water; at room temp. for 5 h;

DOI:10.1039/b309072h

Reference yield:

4-vinylbenzo-18-crown-6 (39557-71-6) + Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol(2-)) (666826-42-2) + N-butylamine (109-73-9,85404-21-3) → [Pd(1,2-bis(bis(4-isopropenylphenyl)phosphane)ethane)(4,6-dinitropyrogallol(3-))](n-butylammonium)-4'-vinylbenzo-18-crown-6

Guidance literature:

In dichloromethane; Pd complex combined with n-butyl amine (1 equiv.) and crown ether (1 equiv.) in CH2Cl2;

DOI:10.1039/b309072h

upstream raw materials:

4,6-dinitropyrogallol

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