ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside
CAS No.:215360-88-6
Molecular Formula:C₃₇H₄₁BrO₅S
Molecular Weight:677.7
Hs Code.:

Synonyms:ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside

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Chemical Property of ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside

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Technology Process of ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside

There total 1 articles about ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 39483-51-7,119645-03-3,128850-50-0,126461-54-9
ethyl 2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside

: 626-15-3
1,3-bis-(bromomethyl)benzene

: 215360-88-6
ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside

Guidance literature:: With 15-crown-5; sodium hydride; In dichloromethane; at -17 ℃; for 8h;
DOI:10.1021/jo990132e

Reference yield: 64.0%

: 215360-88-6
ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside

: 17791-36-5
methyl 2,3-di-O-benzyl-α-D-glucopyranoside

: 215360-97-7
ethyl 6-O-[3-(methyl 2,3-di-O-benzyl-α-D-glucopyranoside-6-yloxymethyl)-benzyl]-2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: methyl 2,3-di-O-benzyl-α-D-glucopyranoside; With di(n-butyl)tin oxide; In toluene; for 3h; Heating;

ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside; With tetra-(n-butyl)ammonium iodide; In toluene; at 90 ℃; for 6h;
DOI:10.1021/jo990132e

Reference yield: 63.0%

: 53685-11-3
(2R,3R,4S,5R,6S)-5-Benzyloxy-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3,4-diol

: 215360-88-6
ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside

: 241471-03-4
ethyl 6-O-[3-(methyl 2,6-di-O-benzyl-α-D-galactopyranoside-3-yloxymethyl)-benzyl]-2,3,4-tri-O-benzyl-1-thio-β-D-glucopyranoside

Guidance literature:: (2R,3R,4S,5R,6S)-5-Benzyloxy-2-benzyloxymethyl-6-methoxy-tetrahydro-pyran-3,4-diol; With di(n-butyl)tin oxide; In toluene; for 5h; Heating;

ethyl 2,3,4-tri-O-benzyl-6-O-(3-bromomethylbenzyl)-1-thio-β-D-glucopyranoside; With tetrabutylammomium bromide; In toluene; at 90 ℃; for 20h;
DOI:10.1021/jo990132e