C₅₄H₅₉N₁₁O₁₆S

Base Information

Chemical Name:C₅₄H₅₉N₁₁O₁₆S
CAS No.:175916-22-0
Molecular Formula:C₅₄H₅₉N₁₁O₁₆S
Molecular Weight:1150.19
Hs Code.:

C<sub>54</sub>H<sub>59</sub>N<sub>11</sub>O<sub>16</sub>S

Synonyms:C₅₄H₅₉N₁₁O₁₆S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₄H₅₉N₁₁O₁₆S

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Technology Process of C₅₄H₅₉N₁₁O₁₆S

There total 13 articles about C₅₄H₅₉N₁₁O₁₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: C₇₀H₇₇N₁₁O₁₆SSi

: 175916-22-0
C₅₄H₅₉N₁₁O₁₆S

Guidance literature:: With pyridine; hydrogen fluoride; for 14h; Ambient temperature;
DOI:10.1021/ja952322m

Reference yield:

: 441044-21-9
Benzoic acid (2R,3S,4R)-4-hydroxy-2-(2-hydroxy-ethyl)-5-methoxy-tetrahydro-furan-3-ylmethyl ester

: 175916-22-0
C₅₄H₅₉N₁₁O₁₆S

Guidance literature:: Multi-step reaction with 8 steps

1: 100 percent / imidazole / tetrahydrofuran

2: 74 percent / pyridine, DMAP

3: 1.) N-methyl-N-(trimethylsilyl)trifluoroacetamide, 2.) trimethylsilyl triflate

4: TBAF / tetrahydrofuran / 4 h / Ambient temperature

5: 75 percent / PPh₃, CBr₄ / acetonitrile / 0.75 h

6: 92 percent / aq. Cs₂CO₃ / tetrahydrofuran / 2.5 h / 35 °C

7: 96 percent / oxone, aq. NaOAc / methanol; tetrahydrofuran / 2 h / Ambient temperature

8: 90 percent / HF, pyridine / 14 h / Ambient temperature

With pyridine; 1H-imidazole; dmap; Oxone; carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; hydrogen fluoride; tetrabutyl ammonium fluoride; sodium acetate; caesium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja952322m

Reference yield:

: 175915-97-6
C₃₈H₄₂O₇Si

: 175916-22-0
C₅₄H₅₉N₁₁O₁₆S

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) N-methyl-N-(trimethylsilyl)trifluoroacetamide, 2.) trimethylsilyl triflate

2: TBAF / tetrahydrofuran / 4 h / Ambient temperature

3: 75 percent / PPh₃, CBr₄ / acetonitrile / 0.75 h

4: 92 percent / aq. Cs₂CO₃ / tetrahydrofuran / 2.5 h / 35 °C

5: 96 percent / oxone, aq. NaOAc / methanol; tetrahydrofuran / 2 h / Ambient temperature

6: 90 percent / HF, pyridine / 14 h / Ambient temperature

With pyridine; Oxone; carbon tetrabromide; trimethylsilyl trifluoromethanesulfonate; N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; hydrogen fluoride; tetrabutyl ammonium fluoride; sodium acetate; caesium carbonate; triphenylphosphine; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja952322m