N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide

Base Information

Chemical Name:N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide
CAS No.:1245904-69-1
Molecular Formula:C₂₃H₁₈N₂O₄Se
Molecular Weight:465.367
Hs Code.:

Synonyms:N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide

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Chemical Property of N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide

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Technology Process of N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide

There total 5 articles about N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 1245904-68-0
N-[5-benzyl-4-(4-methoxyphenyl)-1,3-selenazol-2-yl]-3,4-dimethoxybenzamide

: 1245904-69-1
N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide

Guidance literature:: With boron tribromide; In dichloromethane; at 0 - 20 ℃; for 2h;

Reference yield:

: 645-45-4
hydrocinnamic acid chloride

: 1245904-69-1
N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: aluminum (III) chloride / dichloromethane / 2 h / -5 - 20 °C

2.1: bromine; aluminum (III) chloride / chloroform / 0.5 h / 5 - 20 °C

3.1: CH₃COONH₄/Al₂O₃ / toluene / 24 h / 80 °C

4.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 20 °C

4.2: 20 °C

5.1: boron tribromide / dichloromethane / 2 h / 0 - 20 °C

With aluminum (III) chloride; bromine; boron tribromide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In dichloromethane; chloroform; N,N-dimethyl-formamide; toluene;

Reference yield:

: 106511-71-1
2-Bromo-1-(4'-methoxyphenyl)-3-phenyl-1-propanone

: 1245904-69-1
N-[5-benzyl-4-(4-hydroxyphenyl)-1,3-selenazol-2-yl]-3,4-dihydroxybenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: CH₃COONH₄/Al₂O₃ / toluene / 24 h / 80 °C

2.1: N-ethyl-N,N-diisopropylamine; benzotriazol-1-ol / N,N-dimethyl-formamide / 0.25 h / 20 °C

2.2: 20 °C

3.1: boron tribromide / dichloromethane / 2 h / 0 - 20 °C

With boron tribromide; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; toluene;