C₃₀H₂₅NO₄

Base Information

Chemical Name:C₃₀H₂₅NO₄
CAS No.:137648-63-6
Molecular Formula:C₃₀H₂₅NO₄
Molecular Weight:463.533
Hs Code.:

C<sub>30</sub>H<sub>25</sub>NO<sub>4</sub>

Synonyms:C₃₀H₂₅NO₄

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Chemical Property of C₃₀H₂₅NO₄

Chemical Property:

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Technology Process of C₃₀H₂₅NO₄

There total 7 articles about C₃₀H₂₅NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 137648-52-3,141395-16-6
C₃₀H₂₁NO₃

: 137648-63-6
C₃₀H₂₅NO₄

Guidance literature:: With cyclohexa-1,4-diene; water; toluene-4-sulfonic acid; In benzene; at 25 ℃; for 4h;
DOI:10.1021/ja00071a003

Reference yield:

: 130012-94-1
N-<(phenyloxy)carbonyl>-6a,10a-epoxy-6-ethynyl-10-oxo-5,6,6a,7,8,9,10,10a-octahydrophenanthridine

: 137648-63-6
C₃₀H₂₅NO₄

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / Et₃N, Pd(Ph₃)4, cuprous iodide / benzene / 2 h / 40 °C

2: 84 percent / LiOH*H₂O / tetrahydrofuran; H₂O / 0.67 h / 25 °C

3: 89 percent / lithium diisopropylamide / toluene; cyclohexane / 0.17 h / -78 °C

4: 81 percent / 4-(dimethylamino)pyridine (DMAP) / CH₂Cl₂ / 168 h / 25 °C

5: 94 percent / n-Bu₃SnH, azoisobutyronitrile (AIBN) / toluene / 1 h / 25 °C

6: 79 percent / 1,4-cyclohexadiene, TsOH, H₂O / benzene / 4 h / 25 °C

With dmap; lithium hydroxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2'-azobis(isobutyronitrile); cyclohexa-1,4-diene; water; tri-n-butyl-tin hydride; toluene-4-sulfonic acid; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; cyclohexane; water; toluene; benzene;
DOI:10.1021/ja00071a003

Reference yield:

: 137648-49-8
N-<(phenoxy)carbonyl>-6-<<(2-ethynyl)phenyl>ethynyl>-6a,10a-epoxy-10-oxo-5,6,6a,7,8,9,10,10a-octahydrophenanthridine

: 137648-63-6
C₃₀H₂₅NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / lithium diisopropylamide / toluene; cyclohexane / 0.17 h / -78 °C

2: 81 percent / 4-(dimethylamino)pyridine (DMAP) / CH₂Cl₂ / 168 h / 25 °C

3: 94 percent / n-Bu₃SnH, azoisobutyronitrile (AIBN) / toluene / 1 h / 25 °C

4: 79 percent / 1,4-cyclohexadiene, TsOH, H₂O / benzene / 4 h / 25 °C

With dmap; 2,2'-azobis(isobutyronitrile); cyclohexa-1,4-diene; water; tri-n-butyl-tin hydride; toluene-4-sulfonic acid; lithium diisopropyl amide; In dichloromethane; cyclohexane; toluene; benzene;
DOI:10.1021/ja00071a003