5-[3-chloro-4-(pentafluoro-λ⁶-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole

Base Information

• Chemical Name: 5-[3-chloro-4-(pentafluoro-λ⁶-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole
• CAS No.: 913536-10-4
• Molecular Formula: C₁₃H₁₄ClF₆NOS
• Molecular Weight: 381.77

Synonyms:5-[3-chloro-4-(pentafluoro-λ⁶-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole

Chemical Property of 5-[3-chloro-4-(pentafluoro-λ⁶-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of 5-[3-chloro-4-(pentafluoro-λ⁶-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole

There total 3 articles about 5-[3-chloro-4-(pentafluoro-λ⁶-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

5-chloro-6-(pentafluoro-λ6-sulfanyl)hex-1-ene (860438-41-1) + 4-fluoro-N-hydroxybenzimidoyl chloride (42202-95-9) → 5-[3-chloro-4-(pentafluoro-λ6-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole (913536-10-4)

Guidance literature:

With triethylamine; In diethyl ether; at -20 - -15 ℃;

DOI:10.1055/s-2006-942498

Reference yield:

2-chloro-1,5-hexadiene (101933-88-4) → 5-[3-chloro-4-(pentafluoro-λ6-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole (913536-10-4)

Guidance literature:

Multi-step reaction with 2 steps

1: pentafluorosulfanyl chloride

2: 93 percent / Et₃N / diethyl ether / -20 - -15 °C

With triethylamine; In diethyl ether;

DOI:10.1055/s-2006-942498

Reference yield:

4-fluorobenzaldoxime (459-23-4,7304-35-0) → 5-[3-chloro-4-(pentafluoro-λ6-sulfanyl)butyl]-3-(4-fluorophenyl)-4,5-dihydroisoxazole (913536-10-4)

Guidance literature:

Multi-step reaction with 2 steps

1: N-chlorosuccinimide

2: 93 percent / Et₃N / diethyl ether / -20 - -15 °C

With N-chloro-succinimide; triethylamine; In diethyl ether;

DOI:10.1055/s-2006-942498

upstream raw materials:

5-chloro-6-(pentafluoro-λ⁶-sulfanyl)hex-1-ene

4-fluoro-N-hydroxybenzimidoyl chloride

2-chloro-1,5-hexadiene

4-fluorobenzaldoxime

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