di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate

Base Information

Chemical Name:di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate
CAS No.:1443619-95-1
Molecular Formula:C₂₂H₃₅N₅O₆
Molecular Weight:465.55
Hs Code.:

Synonyms:di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate

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Technology Process of di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate

There total 4 articles about di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1382469-16-0
C₂₂H₃₅BrN₂O₆

: 1443619-95-1
di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate

Guidance literature:: With copper(l) iodide; sodium azide; L-proline; sodium hydroxide; In ethanol; water; at 95 ℃; for 30h;
DOI:10.1021/ml400155a

Reference yield: 59.0%

: 1443619-95-1
di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate

Guidance literature:: With copper(l) iodide; sodium azide; L-proline; sodium hydroxide; In dimethyl sulfoxide; at 90 ℃; for 24h; Inert atmosphere; Sealed tube;

Reference yield:

: 106120-04-1
5-bromoresorcinol

: 1443619-95-1
di-tert-butyl (((5-azido-1,3-phenylene)bis(oxy))bis(propane-3,1-diyl))dicarbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide; water / 0.67 h / 20 - 45 °C

1.2: 29 h / 45 °C

2.1: sodium azide; sodium hydroxide; L-proline; copper(l) iodide / water; ethanol / 30 h / 95 °C

With copper(l) iodide; sodium azide; potassium carbonate; L-proline; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ml400155a