1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide

Base Information

Chemical Name:1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide
CAS No.:1000394-25-1
Molecular Formula:BrH*C₁₃H₁₅N₃O₂S
Molecular Weight:358.259
Hs Code.:

Synonyms:1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide

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Chemical Property of 1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide

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Technology Process of 1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide

There total 3 articles about 1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 816-40-0
1-Bromo-2-butanone

: 360569-98-8
[2-(4-nitrophenyl)-1-(S)-thiocarbamoylethyl]carbamic acid tert-butyl ester

: 1000394-25-1
1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide

Guidance literature:: In acetonitrile; for 3h; Reflux;

Reference yield:

: 33305-77-0
Boc-Phe(p-NO₂)-OH

: 1000394-25-1
1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / N,N-dimethyl-formamide / 0.33 h / 0 °C

1.2: 0.5 h / 0 °C

2.1: Lawessons reagent / tetrahydrofuran / 3 h / 20 °C

3.1: acetonitrile / 3 h / Reflux

With Lawessons reagent; 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 66163-67-5
[1-(S)-carbamoyl-2-(4-nitrophenyl)ethyl]carbamic acid tert-butyl ester

: 1000394-25-1
1-(S)-(4-ethylthiazol-2-yl)-2-(4-nitrophenyl)ethyl amine hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: Lawessons reagent / tetrahydrofuran / 3 h / 20 °C

2: acetonitrile / 3 h / Reflux

With Lawessons reagent; In tetrahydrofuran; acetonitrile;