(4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole

Base Information

Chemical Name:(4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole
CAS No.:154132-43-1
Molecular Formula:C₁₆H₁₅NOS
Molecular Weight:269.367
Hs Code.:

Synonyms:(4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole

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Chemical Property of (4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole

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Technology Process of (4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole

There total 2 articles about (4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 6609-54-7
2-cyanothioanisole

: 20989-17-7
(2S)-2-phenylglycinol

: 154132-43-1
(4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole

Guidance literature:: With zinc(II) chloride; In chlorobenzene; for 48h; Heating;
DOI:10.1016/S0957-4166(00)80417-6

Reference yield:

: N-(2-hydroxy-1-phenyl-ethyl)-2-methylsulfanyl-benzamide

: 154132-43-1
(4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole

Guidance literature:: N-(2-hydroxy-1-phenyl-ethyl)-2-methylsulfanyl-benzamide; With Vilsmeier reagent; In pyridine; at 20 ℃;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pyridine; at 50 ℃; for 3h; Further stages.;
DOI:10.1021/jo000664r

Reference yield: 94.0%

: 56678-60-5
(1,5-cyclooctadiene)bis(pyridine)iridium(I) hexafluorophosphate

: 154132-43-1
(4S)-2-[2-(methylsulfanyl)phenyl]-4-phenyl-4,5-dihydro-1,3-oxazole

: IrCH₃SC₆H₄C₃H₃NOC₆H₅C₈H₁₂NC₅H₅⁽¹⁺⁾*PF₆^(1-)=IrCH₃SC₆H₄C₃H₃NOC₆H₅C₈H₁₂NC₅H₅PF₆

Guidance literature:: In dichloromethane; (Ar); stirring a soln. of ligand and iridium complex in CH2Cl2 for 2 h; addn. of Et2O, filtration, washing ppt. with cold Et2O; elem. anal.;
DOI:10.1016/j.jorganchem.2004.03.015