9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine

Base Information

Chemical Name:9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine
CAS No.:131035-20-6
Molecular Formula:C₁₉H₁₇ClN₂O₂
Molecular Weight:340.809
Hs Code.:

Synonyms:9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine

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Chemical Property of 9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine

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Technology Process of 9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine

There total 1 articles about 9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 104-88-1
4-chlorobenzaldehyde

: 79062-23-0
methyl-6 dihydro-5,6 N-orthoaminophenylamino-4-pyrone-2

: 131035-20-6
9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine

Guidance literature:: With acetic acid; In ethanol; for 72h; Ambient temperature;

Reference yield:

: 131035-20-6
9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine

: N²-benzyl-3-(2-hydroxypropyl)-2-quinoxalinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / sodium hypocloride; water; sulfuric acid / acetonitrile / 2.5 h / 20 °C / pH 5

2: 72 percent / acetic acid / ethyl acetate / 4 h / Heating

With sodium hypochlorite; sulfuric acid; water; acetic acid; In ethyl acetate; acetonitrile;

Reference yield:

: 131035-20-6
9,10-dihydro-9-methyl-7-oxo<3,4-c>pyrano-6-(parachlorophenyl)-(11H)-5,6-dihydrobenzodiazepine

: N²-benzyl-N²-methyl-3-(2-hydroxypropyl)-2-quinoxalinecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / sodium hypocloride; water; sulfuric acid / acetonitrile / 2.5 h / 20 °C / pH 5

2: 65 percent / acetic acid / ethyl acetate / 4 h / Heating

With sodium hypochlorite; sulfuric acid; water; acetic acid; In ethyl acetate; acetonitrile;