iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2

Base Information

Chemical Name:iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2
CAS No.:82247-29-8
Molecular Formula:CH₂Cl₂*C₄₁H₃₄FeO₂P₂S₂
Molecular Weight:846.812
Hs Code.:

Synonyms:iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2

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Chemical Property of iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2

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Technology Process of iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2

There total 5 articles about iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 7608-17-5
2-diphenylphosphino-1-phenylethyne

: 86196-40-9
2P(C₆H₅)3*2CO*CS₂*Fe=(P(C₆H₅)3)2(CO)2(CS₂)Fe

: 82247-29-8
iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2

Guidance literature:: In methanol; diethyl ether; Heating of (PPh3)(CO)2(CS2)Fe and Ph2PCCPh in mixt. of methanol and diethyl ether (N2, reflux, 20 h).; Cooling to room temp., filtration of red ppt., washing (2x) with methanol, drying under vac., recrystn. from CH2Cl2/hexane, elem. anal..;

Reference yield: 74.0%

: 110614-77-2
(chloro)iron(II)(η1-Ph2PCH2C(Ph)S)(η2-SCOMe)(PPh3)(CO)

: 82247-29-8
iron(II)(η2-Ph2PCHC(Ph)S)(η2-SCOMe)(PPh3)(CO)*1.25CH2Cl2

Guidance literature:: With NaHCO₃; In dichloromethane; water; Treatment of Fe-complex with aq. soln. of NaHCO3 under N2.;

Reference yield: 44.0%

: 7608-17-5
2-diphenylphosphino-1-phenylethyne

: bis(triphenylphosphine)(π-carbondisulphide)dicarbonyliron(II)

: 82247-29-8
Fe(CO)(P(C₆H₅)3)((C₆H₅)2PCHCC₆H₅S)(CSOCH₃)

Guidance literature:: With CH₃OH; In methanol; dichloromethane; A soln. of reagents in MeOH-CH2Cl2 was refluxed for 1.5 h (N2 atm.);; chromy. on silica gel thick-layer plates (hexane-ether); crystd. from hexane-CH2Cl2; elem. anal.;;