Technology Process of C11H14N2O2
There total 4 articles about C11H14N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
water; lithium hydroxide;
In
dimethyl sulfoxide;
at 110 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydride / diethyl ether; dimethyl sulfoxide; mineral oil / 3.58 h / 20 - 35 °C
2.1: water; sulfuric acid / 8 h / Reflux
3.1: triethylamine; diphenyl phosphoryl azide / toluene / 1.17 h / 20 - 100 °C
3.2: 3 h / 100 °C
4.1: water; lithium hydroxide / dimethyl sulfoxide / 2 h / 110 °C
With
sulfuric acid; diphenyl phosphoryl azide; water; sodium hydride; triethylamine; lithium hydroxide;
In
diethyl ether; dimethyl sulfoxide; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: triethylamine; diphenyl phosphoryl azide / toluene / 1.17 h / 20 - 100 °C
1.2: 3 h / 100 °C
2.1: water; lithium hydroxide / dimethyl sulfoxide / 2 h / 110 °C
With
diphenyl phosphoryl azide; water; triethylamine; lithium hydroxide;
In
dimethyl sulfoxide; toluene;