3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester

Base Information

• Chemical Name: 3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester
• CAS No.: 1262847-02-8
• Molecular Formula: C₂₀H₂₀N₂O₄
• Molecular Weight: 352.39

Synonyms:3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester

Chemical Property of 3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester

Chemical Property:

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Technology Process of 3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester

There total 4 articles about 3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

dimethyl Isophthalate (1459-93-4) → 3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester (1262847-02-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran

2: N-ethyl-N,N-diisopropylamine; hydrazine

With sodium hydride; N-ethyl-N,N-diisopropylamine; hydrazine; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2011.01.014

Reference yield:

1-<4-(Dimethoxymethyl)phenyl>ethanone (166518-43-0) → 3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester (1262847-02-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydride / tetrahydrofuran

2: N-ethyl-N,N-diisopropylamine; hydrazine

With sodium hydride; N-ethyl-N,N-diisopropylamine; hydrazine; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2011.01.014

Reference yield:

3-[3-(4-dimethoxymethylphenyl)-3-oxopropionyl]benzoic acid methyl ester (1262847-00-6) → 3-[5-(4-dimethoxymethylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester (1262847-02-8)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; hydrazine;

DOI:10.1016/j.bmcl.2011.01.014

upstream raw materials:

3-[3-(4-dimethoxymethylphenyl)-3-oxopropionyl]benzoic acid methyl ester

dimethyl Isophthalate

1-<4-(Dimethoxymethyl)phenyl>ethanone

Downstream raw materials:

3-[5-(4-formylphenyl)-1H-pyrazol-3-yl]benzoic acid methyl ester

3-(5-{4-[(tetrahydropyran-4-ylamino)methyl]phenyl}-1 H-pyrazol-3-yl)benzoic acid methyl ester

N-((R)-cyano-methyl-methyl)-3-{5-[4-(isopropylaminomethyl)phenyl]-1H-pyrazol-3-yl}benzamide

C₂₁H₂₃N₃O₂

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