1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene

Base Information

Chemical Name:1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene
CAS No.:81777-30-2
Molecular Formula:C₂₃H₂₂NO₂P
Molecular Weight:375.407
Hs Code.:

1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ<sup>5</sup>-phosphabuta-1,3-diene

Synonyms:1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene

There total 3 articles about 1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 81777-19-7
(E)-3-azido-but-2-enoic acid methyl ester

: 603-35-0
triphenylphosphine

: 81777-30-2
1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene

Guidance literature:: DOI:10.1016/S0040-4039(00)79357-9

Reference yield:

: 623-43-8
crotonic acid methyl ester

: 81777-30-2
1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene

Guidance literature:: Multi-step reaction with 3 steps

1: 45 percent / iodine(I) azide / acetonitrile / 24 h

2: 96 percent / 1,4-diazabicyclo<2.2.2>octane / acetone / 24 h / 20 °C

3: 42 percent / CH₂Cl₂ / 1 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; iodine(I) azide; In dichloromethane; acetone; acetonitrile;

Reference yield:

: methyl erythro-3-azido-2-iodo-butanoate

: 81777-30-2
1,1,1-Triphenyl-3-methyl-4-(methoxycarbonyl)-2-aza-1λ⁵-phosphabuta-1,3-diene

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / 1,4-diazabicyclo<2.2.2>octane / acetone / 24 h / 20 °C

2: 42 percent / CH₂Cl₂ / 1 h / 20 °C

With 1,4-diaza-bicyclo[2.2.2]octane; In dichloromethane; acetone;