Technology Process of methyl 2-phenylselenenyloctadecanoate
There total 2 articles about methyl 2-phenylselenenyloctadecanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: bromine / tetrahydrofuran
2: 1.) lithium diisopropylamide / 1.) THF, -50 deg C, 1 h, 2.) -50 deg C -> room temperature, 30 min
With
bromine; lithium diisopropyl amide;
In
tetrahydrofuran;
DOI:10.1021/ja00404a023
- Guidance literature:
-
With
lithium diisopropyl amide;
Yield given. Multistep reaction;
1.) THF, -50 deg C, 1 h, 2.) -50 deg C -> room temperature, 30 min;
DOI:10.1021/ja00404a023
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) lithium diisopropylamide, 2.) hydrogen peroxide, acetic acid / 1.) THF, -78 deg C, 20 min, 2.) 0 deg C, 30 min, room temperature, 2 h
2: 98 percent / KOH / methanol; H2O / 2 h / 25 °C
3: 50 percent / CH2Cl2 / Ambient temperature
With
potassium hydroxide; dihydrogen peroxide; acetic acid; lithium diisopropyl amide;
In
methanol; dichloromethane; water;
DOI:10.1021/ja00404a023
