3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate

Base Information

Chemical Name:3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate
CAS No.:114894-72-3
Molecular Formula:C₇H₈O₃S*C₉H₁₅NO₄
Molecular Weight:373.427
Hs Code.:

Synonyms:3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate

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Chemical Property of 3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate

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Technology Process of 3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate

There total 6 articles about 3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 22169-72-8
3-azido-3-deoxy-6-O-toluene-p-sulphonyl-1,2-O-isopropylidene-α-D-glucofuranose

: 114894-72-3
3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate

Guidance literature:: With hydrogen; palladium; In ethanol; for 24h;
DOI:10.1016/S0040-4020(01)86851-4

Reference yield:

: 14686-89-6
(1,2:5,6)-di-O-isopropylidene-D-gulose

: 114894-72-3
3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate

Guidance literature:: Multi-step reaction with 5 steps

1: pyridine / CH₂Cl₂ / 0.5 h / -30 °C

2: sodium azide / dimethylformamide / 8 h / 50 °C

3: 100 percent / acetic acid / methanol; H₂O / 12 h / 50 °C

4: 89 percent / pyridine / 24 h / -10 °C

5: 77 percent / hydrogen / palladium black / ethanol / 24 h

With pyridine; sodium azide; hydrogen; acetic acid; palladium; In methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(01)86851-4

Reference yield:

: 13964-23-3
3-azido-3-deoxy-1,2:5,6-di-(O-isopropylidene)-α-D-glucofuranose

: 114894-72-3
3,6-dideoxy-3,6-imino-1,2-O-isopropylidene-α-D-glucofuranose p-toluenesulphonate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / acetic acid / methanol; H₂O / 12 h / 50 °C

2: 89 percent / pyridine / 24 h / -10 °C

3: 77 percent / hydrogen / palladium black / ethanol / 24 h

With pyridine; hydrogen; acetic acid; palladium; In methanol; ethanol; water;
DOI:10.1016/S0040-4020(01)86851-4