acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester

Base Information

Chemical Name:acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester
CAS No.:1445651-38-6
Molecular Formula:C₁₆H₁₇NO₆
Molecular Weight:319.314
Hs Code.:

Synonyms:acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester

Chemical Property:

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Technology Process of acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester

There total 3 articles about acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15568-85-1
5-methoxymethylene-2,2-dimethyl-1,3-dioxane-4,6-dione

: 154396-34-6
acetic acid 4-amino-2-methylphenyl ester

: 1445651-38-6
acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester

Guidance literature:: In ethanol; at 70 ℃; for 0.5h;

Reference yield:

: 99-53-6
2-methyl-4-nitrophenol

: 1445651-38-6
acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: pyridine / dichloromethane / 2 h / 0 - 20 °C

2.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 18 h / 20 °C

2.2: Ra-Ni / 6 h

3.1: ethanol / 0.5 h / 70 °C

With pyridine; palladium on activated charcoal; hydrogen; In tetrahydrofuran; ethanol; dichloromethane;

Reference yield:

: 67141-99-5
acetic acid 2-methyl-4-nitrophenyl ester

: 1445651-38-6
acetic acid 4-[(2,2-dimethyl-4,6-dioxo-[1,3]dioxan-5-ylidene methyl)amino]-2-methylphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 18 h / 20 °C

1.2: Ra-Ni / 6 h

2.1: ethanol / 0.5 h / 70 °C

With palladium on activated charcoal; hydrogen; In tetrahydrofuran; ethanol;