2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine

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Chemical Name:2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine
CAS No.:1210405-82-5
Molecular Formula:C₂₆H₄₂N₂
Molecular Weight:382.633
Hs Code.:

Synonyms:2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine

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Chemical Property of 2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine

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Technology Process of 2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine

There total 4 articles about 2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.48%

: 111-86-4
n-Octylamine

: 1210405-73-4
2-((2,6-bis(1-methylethyl)phenyl)amino)-2-cyclohexen-1-one

: 1210405-82-5
2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine

Guidance literature:: With formic acid; In toluene; at 75 ℃; Molecular sieve;
DOI:10.1021/om101207a

Reference yield:

: 765-87-7
cyclohexane-1,2-dione

: 1210405-82-5
2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 5 h / Inert atmosphere; Dean-Stark trap; Reflux

2: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Heating

3: formic acid / toluene / 75 °C / Molecular sieve

With formic acid; toluene-4-sulfonic acid; In toluene;
DOI:10.1021/om101207a

Reference yield:

: 23740-64-9
2-morpholinocyclohex-2-enone

: 1210405-82-5
2,6-bis(1-methylethyl)-N-[(1E)-2-(octylamino)-2-cyclohexen-1-ylidene]benzenamine

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / toluene / 2 h / Inert atmosphere; Heating

2: formic acid / toluene / 75 °C / Molecular sieve

With formic acid; toluene-4-sulfonic acid; In toluene;
DOI:10.1021/om101207a