2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

Base Information

Chemical Name:2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose
CAS No.:116594-36-6
Molecular Formula:C₆₂H₆₄O₁₁
Molecular Weight:985.184
Hs Code.:

Synonyms:2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

Suppliers and Price of 2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

There total 1 articles about 2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.5%

: 67693-18-9
2,3,2',3',4',6'-hexa-O-benzyl-α,α-trehalose

: 4316-35-2
acetophenone dimethyl acetal

: 116594-36-6
2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

Guidance literature:: With toluene-4-sulfonic acid; for 0.0833333h; Ambient temperature;
DOI:10.1016/0008-6215(88)84146-6

Reference yield: 86.8%

: 116594-36-6
2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

: 116594-38-8
2,3,2',3',4',6'-hexa-O-benzyl-6-O-(1-phenylethyl)-α,α-trehalose

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; dichloromethane; for 2h; Heating;
DOI:10.1016/0008-6215(88)84146-6

Reference yield:

: 116594-36-6
2,3,2',3',4',6'-hexa-O-benzyl-4,6-O-(S)-(1-phenylethylidene)-α,α-trehalose

: 116594-39-9
O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1-4)-2,3-di-O-benzyl-6-O-(1-phenylethyl)-α-D-glucopyranosyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86.8 percent / LiAlH₄, AlCl₃ / diethyl ether; CH₂Cl₂ / 2 h / Heating

2: 65 percent / HgBr₂, molecular sieves (4 A) / CH₂Cl₂ / Ambient temperature

With lithium aluminium tetrahydride; aluminium trichloride; 4 A molecular sieve; mercury dibromide; In diethyl ether; dichloromethane;
DOI:10.1016/0008-6215(88)84146-6