C₄₁H₅₆O₈

Base Information

Chemical Name:C₄₁H₅₆O₈
CAS No.:104307-08-6
Molecular Formula:C₄₁H₅₆O₈
Molecular Weight:676.891
Hs Code.:

C<sub>41</sub>H<sub>56</sub>O<sub>8</sub>

Synonyms:C₄₁H₅₆O₈

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Chemical Property of C₄₁H₅₆O₈

Chemical Property:

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Technology Process of C₄₁H₅₆O₈

There total 21 articles about C₄₁H₅₆O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104307-07-5
C₅₇H₇₄O₈Si

: 104307-08-6
C₄₁H₅₆O₈

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; acetonitrile;
DOI:10.1016/S0040-4039(00)84149-0

Reference yield:

: 1250256-05-3
C₄₉H₆₄O₉

: 104307-08-6
C₄₁H₅₆O₈

Guidance literature:: With ammonium cerium (IV) nitrate; In acetonitile; water; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol101833h

Reference yield:

: 104307-04-2
C₅₁H₇₀O₁₀Si

: 104307-08-6
C₄₁H₅₆O₈

Guidance literature:: Multi-step reaction with 8 steps

1: sodium borohydride / ethanol / 1 h / 0 °C / further reag.: LiAlH₄, Zn(BH₄), DIBAL, B₂H₆

2: pyridinium p-toluolsulfonate / CH₂Cl₂ / Ambient temperature

3: hydrogen / palladium hydroxide on carbom / ethyl acetate / 6 h

4: 1) DMSO, oxalyl chloride, 2) triethylamine / 1) CH₂Cl₂, - 78 deg C 2) CH₂Cl₂, -78 to 0 deg C

5: 1)n-butyllithium / 1) THF, RT, 30 min, 2) THF, -78 deg C then reflux, 2 h

6: trimethylbromosilane / CH₂Cl₂ / 1) -78 deg C, 15 min, 2) -25 deg C, 30 min.

7: 60percent sodium hydride / tetrahydrofuran; dimethylformamide / 16 h / Ambient temperature

8: n-Bu₄NF / tetrahydrofuran; acetonitrile / Ambient temperature

With sodium tetrahydroborate; n-butyllithium; oxalyl dichloride; trimethylsilyl bromide; tetrabutyl ammonium fluoride; hydrogen; pyridinium p-toluenesulfonate; sodium hydride; dimethyl sulfoxide; triethylamine; palladium hydroxide - carbon; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/S0040-4020(01)86918-0