tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Base Information

Chemical Name:tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid
CAS No.:120312-11-0
Molecular Formula:C₅₀H₆₄N₆O₁₁Si
Molecular Weight:953.177
Hs Code.:

tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Synonyms:tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

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Chemical Property of tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

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Technology Process of tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

There total 4 articles about tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 99049-62-4
2-azido-2-deoxy-3,4,6-tri-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 120312-04-1
tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

: 120312-11-0
tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Guidance literature:: With boron trifluoride diethyl etherate; In hexane; dichloromethane; at -20 ℃; for 8h;

Reference yield:

: 17674-16-7
benzyl triflate

: 120312-11-0
tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 2,6-di-tert-butylpyridine; 2.) pyridine / 1.) CH₂CL₂, -65 deg C, 20 h; 2.) H₂O, 20 deg C

2: 78 percent / 0.1M BF₃*Et₂O / CH₂Cl₂; hexane / 8 h / -20 °C

With pyridine; 2,6-di-tert-butyl-pyridine; boron trifluoride diethyl etherate; In hexane; dichloromethane;

Reference yield:

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 120312-11-0
tert-Butyldimethylsilyl-2-azido-4-O-(2-azido-3,4,6-tri-O-benzyl-2-desoxy-β-D-glucopyranosyl)-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 1.4 g / CF₃SO₃H / benzene / 12 h / 0 °C

2: 78 percent / 0.1M BF₃*Et₂O / CH₂Cl₂; hexane / 8 h / -20 °C

With trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; In hexane; dichloromethane; benzene;