1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

Base Information

Chemical Name:1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide
CAS No.:1392835-22-1
Molecular Formula:C₂F₆NO₄S₂*C₂₃H₂₀Br₂N₃
Molecular Weight:778.389
Hs Code.:

Synonyms:1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

Suppliers and Price of 1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

There total 4 articles about 1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1392835-23-2
1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium trifluoromethanesulfonate

: 90076-65-6
bis(trifluoromethane)sulfonimide lithium

: 1392835-22-1
1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

Guidance literature:: In chloroform; water; at 20 ℃; for 3h;
DOI:10.1016/j.electacta.2012.05.049

Reference yield:

: 81090-53-1
N,N-bis(4-bromophenyl)aniline

: 1392835-22-1
1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

Guidance literature:: Multi-step reaction with 4 steps

1.1: trichlorophosphate / 1 h / 95 °C

1.2: 0.5 h

2.1: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; ethanol / 1 h / 20 °C

3.1: dichloromethane / 2 h / 0 °C

4.1: chloroform; water / 3 h / 20 °C

With sodium tetrahydroborate; sodium hydroxide; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; 1.1: Vilsmeier-Haack reaction;
DOI:10.1016/j.electacta.2012.05.049

Reference yield:

: 25069-38-9
N,N-bis(4-bromophenyl)aminobenzaldehyde

: 1392835-22-1
1-{4-[bis(4-bromophenyl)amino]benzyl}-3-methylimidazolium bis(trifluoromethanesulfonyl)amide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; sodium hydroxide / tetrahydrofuran; ethanol / 1 h / 20 °C

2: dichloromethane / 2 h / 0 °C

3: chloroform; water / 3 h / 20 °C

With sodium tetrahydroborate; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water;
DOI:10.1016/j.electacta.2012.05.049