C₄₄H₆₉N₃O₃

Base Information

• Chemical Name: C₄₄H₆₉N₃O₃
• CAS No.: 1242190-06-2
• Molecular Formula: C₄₄H₆₉N₃O₃
• Molecular Weight: 688.05
• Mol file: 1242190-06-2.mol

Synonyms:C₄₄H₆₉N₃O₃

Chemical Property of C₄₄H₆₉N₃O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₄₄H₆₉N₃O₃

There total 5 articles about C₄₄H₆₉N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

C44H71NO3 (957996-23-5) → C44H69N3O3 (1242190-06-2)

Guidance literature:

C₄₄H₇₁NO₃; With tetrafluoroboric acid; sodium nitrite; In water; Cooling;

With sodium azide; In methanol; at 20 ℃; Cooling with ice;

DOI:10.1039/b9nj00744j

Reference yield:

C44H69NO5 (957996-22-4) → C44H69N3O3 (1242190-06-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: tin(II) chloride dihdyrate / ethyl acetate / Reflux

2.1: tetrafluoroboric acid; sodium nitrite / water / Cooling

2.2: 20 °C / Cooling with ice

With tetrafluoroboric acid; tin(II) chloride dihdyrate; sodium nitrite; In water; ethyl acetate;

DOI:10.1039/b9nj00744j

Reference yield:

11-bromoundecanoyl chloride (15949-84-5) → C44H69N3O3 (1242190-06-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: pyridine / tetrahydrofuran / 12 h / 20 °C

2.1: acetone / 12 h / Reflux

3.1: tin(II) chloride dihdyrate / ethyl acetate / Reflux

4.1: tetrafluoroboric acid; sodium nitrite / water / Cooling

4.2: 20 °C / Cooling with ice

With pyridine; tetrafluoroboric acid; tin(II) chloride dihdyrate; sodium nitrite; In tetrahydrofuran; water; ethyl acetate; acetone;

DOI:10.1039/b9nj00744j

upstream raw materials:

C₄₄H₆₉NO₅

C₄₄H₇₁NO₃

11-bromoundecanoyl chloride

cholesterol

Downstream raw materials:

C₅₂H₇₅N₃O₃

C₅₉H₈₁N₃O₄