(2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol

Base Information

Chemical Name:(2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol
CAS No.:167640-29-1
Molecular Formula:C₃₄H₃₂O₂
Molecular Weight:472.627
Hs Code.:

(2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2<sup>C(6)</sup>,3<sup>C(8)</sup>-dimethanol

Synonyms:(2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol

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Chemical Property of (2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol

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Technology Process of (2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol

There total 2 articles about (2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: phenylmagnesium chloride

: 40335-59-9
dimethyl (2S,3S)-bicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dicarboxylate

: 167640-29-1
(2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol

Guidance literature:: In tetrahydrofuran;
DOI:10.1002/hlca.19940770802

Reference yield:

: 167640-38-2
(1S,2S,3S,4R)-Bicyclo[2.2.2]oct-5-ene-2,3-dicarboxylic acid bis-((1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl) ester

: 167640-29-1
(2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / MeSO₃H / 336 h / 60 °C

2: 83 percent / tetrahydrofuran

With methanesulfonic acid; In tetrahydrofuran;
DOI:10.1002/hlca.19940770802

Reference yield: 90.0%

: 167640-29-1
(2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>oct-5-ene-2^C(6),3^C(8)-dimethanol

: (2S,3S)-α,α,α',α'-tetraphenylbicyclo<2.2.2>octan-2^C(6),3^C(8)-dimethanol

Guidance literature:: With hydrogen; palladium on activated charcoal; In diethyl ether; for 2h; Ambient temperature;
DOI:10.1002/hlca.19940770802