[(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester

Base Information

• Chemical Name: [(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester
• CAS No.: 176660-85-8
• Molecular Formula: C₁₉H₂₆N₂O₅
• Molecular Weight: 362.426

Synonyms:[(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester

Chemical Property of [(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester

Chemical Property:

Purity/Quality:

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Technology Process of [(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester

There total 1 articles about [(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

(R)-4-[(R)-(Benzyl-hydroxy-amino)-furan-2-yl-methyl]-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester → [(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester (176660-85-8)

Guidance literature:

With toluene-4-sulfonic acid; In water; Heating;

DOI:10.1021/jo9714775

Reference yield: 100.0%

acetic anhydride (108-24-7) + [(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester (176660-85-8) → C23H30N2O7 (212330-30-8)

Guidance literature:

With pyridine; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1021/jo9714775

Reference yield:

[(1R,2R)-2-(Benzyl-hydroxy-amino)-2-furan-2-yl-1-hydroxymethyl-ethyl]-carbamic acid tert-butyl ester (176660-85-8) → methyl (2R,3R)-4-acetoxy-2-(N-acetoxy-N-benzylamino)-3-[(tert-butoxycarbonyl)amino]butanoate

Guidance literature:

Multi-step reaction with 3 steps

1: 100 percent / pyridine / CH₂Cl₂ / 1 h / Ambient temperature

2: NaIO₄, RuCl₃*H₂O / acetonitrile; CCl₄; H₂O / 0.08 h

3: diethyl ether

With pyridine; ruthenium trichloride; sodium periodate; In tetrachloromethane; diethyl ether; dichloromethane; water; acetonitrile;

DOI:10.1021/jo9714775

Downstream raw materials:

C₂₃H₃₀N₂O₇

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