Technology Process of 2,3,4,5-tetra-O-methyl-6-O-triphenylmethyl-D-glucose
There total 7 articles about 2,3,4,5-tetra-O-methyl-6-O-triphenylmethyl-D-glucose which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
mercury(II) perchlorate; calcium carbonate;
In
tetrahydrofuran; water;
at 20 ℃;
for 5h;
DOI:10.1016/S0008-6215(02)00528-1
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 32 percent / pyridine / 24 h / Ambient temperature
2: 85 percent / imidazole / CH2Cl2 / 24 h
3: 1.) NaH / 1.) THF, 10 min, 2.) THF, RT, overnight
4: 93 percent / Bu4NF / tetrahydrofuran / Ambient temperature
5: 1.) NMO, 4 A sieves, 2.) tetrapropylammonium perruthenate (TPAP) / 1.) CH2Cl2, 2.) CH2Cl2, RT, 40 min
With
pyridine; 1H-imidazole; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 87 percent / NaBH4 / ethanol
2: 32 percent / pyridine / 24 h / Ambient temperature
3: 85 percent / imidazole / CH2Cl2 / 24 h
4: 1.) NaH / 1.) THF, 10 min, 2.) THF, RT, overnight
5: 93 percent / Bu4NF / tetrahydrofuran / Ambient temperature
6: 1.) NMO, 4 A sieves, 2.) tetrapropylammonium perruthenate (TPAP) / 1.) CH2Cl2, 2.) CH2Cl2, RT, 40 min
With
pyridine; 1H-imidazole; sodium tetrahydroborate; N-methyl-2-indolinone; tetrapropylammonium perruthennate; 4 A molecular sieve; tetrabutyl ammonium fluoride; sodium hydride;
In
tetrahydrofuran; ethanol; dichloromethane;
