(2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde

Base Information

Chemical Name:(2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde
CAS No.:226416-54-2
Molecular Formula:C₁₃H₂₃NO₂
Molecular Weight:225.331
Hs Code.:

Synonyms:(2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde

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Technology Process of (2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde

There total 1 articles about (2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 203176-14-1
ethyl (2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyrate

: 226416-54-2
(2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 2h;
DOI:10.1016/S0040-4020(99)00148-9

Reference yield:

: 226416-54-2
(2R,3S)-2,3-(N,O-isopropylidene)-3-amino-4-cyclohexyl-2-hydroxybutyraldehyde

: 122621-77-6
(2S,3R,4S)-2-amino-1-cyclohexyl-3,4-dihydroxy-6-methylheptane

Guidance literature:: Multi-step reaction with 2 steps

1: 0.57 g / tetrahydrofuran / 6 h / Ambient temperature

2: 52 percent / 6N HCl / methanol / 6 h / Ambient temperature

With hydrogenchloride; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4020(99)00148-9