pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide

Base Information

Chemical Name:pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide
CAS No.:128911-06-8
Molecular Formula:C₂₁H₂₉NO₆
Molecular Weight:391.464
Hs Code.:

Synonyms:pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide

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Chemical Property of pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide

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Technology Process of pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide

There total 1 articles about pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 128911-06-8
pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide

Guidance literature:: In acetic acid; at 100 ℃; for 0.0833333h;
DOI:10.1016/S0040-4020(01)97582-9

Reference yield:

: 128911-06-8
pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide

: 128911-08-0
pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)(2-benzyloxyethan)imine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂OH*HCl, NaHCO₃,AcOH / methanol / 4 h / ultra sonic bath

2: 68 percent / CHCl₃ / 0.17 h / Ambient temperature

With hydroxylamine hydrochloride; sodium hydrogencarbonate; acetic acid; In methanol; chloroform;
DOI:10.1016/S0040-4020(01)97582-9

Reference yield:

: 128911-06-8
pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)-(4-methoxyphenyl)methanimine N-oxide

: 128911-03-5,129263-79-2
pseudo-N-(2,3:5,6-di-O-isopropylidene-α-D-mannofuranosyl)phenylmethanimine N-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: NH₂OH*HCl, NaHCO₃,AcOH / methanol / 4 h / ultra sonic bath

2: 59 percent / CHCl₃ / 6 h / Ambient temperature

With hydroxylamine hydrochloride; sodium hydrogencarbonate; acetic acid; In methanol; chloroform;
DOI:10.1016/S0040-4020(01)97582-9