C₃₇H₇₂N₄O₅SSi₃

Base Information

Chemical Name:C₃₇H₇₂N₄O₅SSi₃
CAS No.:1349053-57-1
Molecular Formula:C₃₇H₇₂N₄O₅SSi₃
Molecular Weight:769.325
Hs Code.:

C<sub>37</sub>H<sub>72</sub>N<sub>4</sub>O<sub>5</sub>SSi<sub>3</sub>

Synonyms:C₃₇H₇₂N₄O₅SSi₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₇H₇₂N₄O₅SSi₃

Chemical Property:

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Technology Process of C₃₇H₇₂N₄O₅SSi₃

There total 19 articles about C₃₇H₇₂N₄O₅SSi₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1349054-48-3
C₃₇H₇₂N₄O₃SSi₃

: 1349053-57-1
C₃₇H₇₂N₄O₅SSi₃

Guidance literature:: With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1021/ol2024746

Reference yield:

: C₁₄H₁₈O₃S

: 1349053-57-1
C₃₇H₇₂N₄O₅SSi₃

Guidance literature:: Multi-step reaction with 17 steps

1.1: tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 4.17 h / 25 °C

2.1: 1H-imidazole / 1,2-dichloro-ethane / 0 - 25 °C / Inert atmosphere

3.1: trimethylaluminum; N-ethyl-N,N-diisopropylamine / hexane; dichloromethane / 2 h / -78 - 25 °C / Inert atmosphere

4.1: toluene / 0.25 h / 0 °C

4.2: 0.08 h / 0 °C

4.3: 20 °C

5.1: dichloromethane / 0.17 h / 0 °C / Inert atmosphere

5.2: 2 h / 0 °C / Inert atmosphere

6.1: toluene / 1 h / 50 - 60 °C

7.1: tetrahydrofuran; toluene / 25 °C / Inert atmosphere

8.1: dichloromethane / 0.25 h / 0 °C

8.2: 0 °C

9.1: methanol / 0.5 h

9.2: 2 h / 0 °C

10.1: ozone / ethyl acetate / 0.5 h / 40 °C

10.2: 8 h / 20 °C / Inert atmosphere

10.3: 0.5 h / Inert atmosphere

11.1: bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine / dichloromethane / 1.5 h / Inert atmosphere

12.1: isopropylmagnesium chloride / tetrahydrofuran / 2 h / -15 - -10 °C / Inert atmosphere

13.1: 1H-imidazole / 1,2-dichloro-ethane / 6 h / 0 - 80 °C / Inert atmosphere

14.1: diisobutylaluminium hydride / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

15.1: borane tert-butylamine / ethanol / 1 h / -78 - 25 °C

15.2: 0 °C

16.1: 2,6-dimethylpyridine / dichloromethane / 4 h / -73 - -60 °C / Inert atmosphere

17.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C

With 1H-imidazole; bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; 2,6-dimethylpyridine; methanol; trimethylaluminum; isopropylmagnesium chloride; diisobutylaluminium hydride; borane tert-butylamine; sodium hydrogencarbonate; ozone; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; toluene; 4.1: Noyori oxidation / 4.2: Noyori oxidation / 4.3: Noyori oxidation / 5.1: Jacobsen epoxidation / 5.2: Jacobsen epoxidation;
DOI:10.1021/ol2024746

Reference yield:

: 1349053-71-9
C₂₀H₂₂O₃S₂

: 1349053-57-1
C₃₇H₇₂N₄O₅SSi₃

Guidance literature:: Multi-step reaction with 16 steps

1.1: 1H-imidazole / 1,2-dichloro-ethane / 0 - 25 °C / Inert atmosphere

2.1: trimethylaluminum; N-ethyl-N,N-diisopropylamine / hexane; dichloromethane / 2 h / -78 - 25 °C / Inert atmosphere

3.1: toluene / 0.25 h / 0 °C

3.2: 0.08 h / 0 °C

3.3: 20 °C

4.1: dichloromethane / 0.17 h / 0 °C / Inert atmosphere

4.2: 2 h / 0 °C / Inert atmosphere

5.1: toluene / 1 h / 50 - 60 °C

6.1: tetrahydrofuran; toluene / 25 °C / Inert atmosphere

7.1: dichloromethane / 0.25 h / 0 °C

7.2: 0 °C

8.1: methanol / 0.5 h

8.2: 2 h / 0 °C

9.1: ozone / ethyl acetate / 0.5 h / 40 °C

9.2: 8 h / 20 °C / Inert atmosphere

9.3: 0.5 h / Inert atmosphere

10.1: bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; triphenylphosphine / dichloromethane / 1.5 h / Inert atmosphere

11.1: isopropylmagnesium chloride / tetrahydrofuran / 2 h / -15 - -10 °C / Inert atmosphere

12.1: 1H-imidazole / 1,2-dichloro-ethane / 6 h / 0 - 80 °C / Inert atmosphere

13.1: diisobutylaluminium hydride / dichloromethane / 0.17 h / -78 °C / Inert atmosphere

14.1: borane tert-butylamine / ethanol / 1 h / -78 - 25 °C

14.2: 0 °C

15.1: 2,6-dimethylpyridine / dichloromethane / 4 h / -73 - -60 °C / Inert atmosphere

16.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 12 h / 20 °C

With 1H-imidazole; bis(4-chlorobenzyl) diazene-1,2-dicarboxylate; 2,6-dimethylpyridine; methanol; trimethylaluminum; isopropylmagnesium chloride; diisobutylaluminium hydride; borane tert-butylamine; sodium hydrogencarbonate; ozone; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; toluene; 3.1: Noyori oxidation / 3.2: Noyori oxidation / 3.3: Noyori oxidation / 4.1: Jacobsen epoxidation / 4.2: Jacobsen epoxidation;
DOI:10.1021/ol2024746