Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Base Information

Chemical Name:Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester
CAS No.:321747-89-1
Molecular Formula:C₁₈H₂₃O₆P
Molecular Weight:366.351
Hs Code.:

Synonyms:Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

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Chemical Property of Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

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Technology Process of Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

There total 4 articles about Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7284-07-3
5,6-dideoxy-1,2-O-isopropylidene-α-D-xylo-hex-5-eno-furanose

: 321747-89-1
Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / tetrahydrofuran

2: t-BuOOH

With 1H-tetrazole; tert.-butylhydroperoxide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)01511-2

Reference yield:

: 1026674-28-1
C₁₅H₂₄NOP

: 321747-89-1
Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / tetrahydrofuran

2: t-BuOOH

With 1H-tetrazole; tert.-butylhydroperoxide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)01511-2

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 321747-89-1
Vinyl-phosphonic acid benzyl ester (3aR,5R,6S,6aR)-2,2-dimethyl-5-vinyl-tetrahydro-furo[2,3-d][1,3]dioxol-6-yl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole / tetrahydrofuran

2: 1H-tetrazole / tetrahydrofuran

3: t-BuOOH

With 1H-tetrazole; tert.-butylhydroperoxide; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)01511-2