1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose

Base Information

Chemical Name:1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose
CAS No.:1019983-66-4
Molecular Formula:C₂₃H₃₀N₅O₇PS
Molecular Weight:551.56
Hs Code.:

Synonyms:1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose

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Chemical Property of 1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose

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Technology Process of 1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose

There total 3 articles about 1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849778-81-0
1-(adenin-9-yl)-3-O-(diisopropylphosphonomethyl)-L-threose

: 1005-56-7
phenylcarbonochloridothioate

: 1019983-66-4
1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose

Guidance literature:: dmap; In acetonitrile; at 20 ℃; for 12h;
DOI:10.1021/ja043045z

Reference yield:

: C₂₅H₃₁O₉P

: 1019983-66-4
1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / SnCl₄ / acetonitrile / 5 h / 20 °C

2: 84 percent / ammonia / methanol / 20 °C

3: DMAP / acetonitrile / 12 h / 20 °C

With ammonia; tin(IV) chloride; dmap; In methanol; acetonitrile;
DOI:10.1021/ja043045z

Reference yield:

: 849778-77-4
1'α-(N⁶-benzoyladenin-9-yl)-2'-O-benzoyl-3'-O-diisopropyl-phosphonomethyl-L-threose

: 1019983-66-4
1-(adenin-9-yl)-2-O-phenoxythiocarbonyl-3-O-(diisopropylphosphonomethyl)-L-threose

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / ammonia / methanol / 20 °C

2: DMAP / acetonitrile / 12 h / 20 °C

With ammonia; dmap; In methanol; acetonitrile;
DOI:10.1021/ja043045z