carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester

Base Information

Chemical Name:carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester
CAS No.:524938-82-7
Molecular Formula:C₁₆H₁₈O₆
Molecular Weight:306.315
Hs Code.:

Synonyms:carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester

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Chemical Property of carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester

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Technology Process of carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester

There total 2 articles about carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 79-22-1
methyl chloroformate

: 524938-81-6
3,4-dihydroxy-allylbenzene

: 524938-82-7
carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester

Guidance literature:: With pyridine; In dichloromethane; at 0 - 25 ℃;
DOI:10.1081/CAR-120016853

Reference yield:

: 643-79-8
o-phthalic dicarboxaldehyde

: 524938-82-7
carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 35 percent / tetrahydrofuran / 16 h

2: 55 percent / pyridine / CH₂Cl₂ / 0 - 25 °C

With pyridine; In tetrahydrofuran; dichloromethane;
DOI:10.1081/CAR-120016853

Reference yield: 63.0%

: 1199614-81-7
2,3,5-tri-O-acetyl-D-ribofuranose

: 524938-82-7
carbonic acid 1-[2-(1-methoxycarbonyloxy-allyl)-phenyl]-allyl ester methyl ester

: 1,2-bis[(E)-3-(2,3,5-tri-O-acetyl-D-ribofuranosyloxy)prop-1-en-1-yl]benzene

Guidance literature:: With 1,4-di(diphenylphosphino)-butane; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; In tetrahydrofuran; at 60 ℃;
DOI:10.1081/CAR-120016853