Technology Process of C28H28Cl2N6O
There total 8 articles about C28H28Cl2N6O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lead cyanamide;
In
N,N-dimethyl-formamide;
at 140 ℃;
for 2h;
microwave irradiation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydrogencarbonate / acetonitrile / 0.25 h / 20 °C / cooled on a water bath
2: hydrogen / palladium 10% on activated carbon / methanol
3: tetrahydrofuran / 18 h / 20 °C
4: lead cyanamide / N,N-dimethyl-formamide / 2 h / 140 °C / microwave irradiation
With
hydrogen; sodium hydrogencarbonate;
palladium 10% on activated carbon;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: thiophene; hydrogen / platinum on carbon / tetrahydrofuran; methanol / 20 °C
2: sodium hydrogencarbonate / acetonitrile / 0.25 h / 20 °C / cooled on a water bath
3: hydrogen / palladium 10% on activated carbon / methanol
4: tetrahydrofuran / 18 h / 20 °C
5: lead cyanamide / N,N-dimethyl-formamide / 2 h / 140 °C / microwave irradiation
With
thiophene; hydrogen; sodium hydrogencarbonate;
palladium 10% on activated carbon; platinum on carbon;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetonitrile;