C₃₄H₄₆N₂O₇

Base Information

Chemical Name:C₃₄H₄₆N₂O₇
CAS No.:1543006-58-1
Molecular Formula:C₃₄H₄₆N₂O₇
Molecular Weight:594.748
Hs Code.:

C<sub>34</sub>H<sub>46</sub>N<sub>2</sub>O<sub>7</sub>

Synonyms:C₃₄H₄₆N₂O₇

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Chemical Property of C₃₄H₄₆N₂O₇

Chemical Property:

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Technology Process of C₃₄H₄₆N₂O₇

There total 13 articles about C₃₄H₄₆N₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1586795-33-6
C₁₉H₂₇NO₅

: C₁₅H₂₁NO₃*C₂HF₃O₂

: 1543006-58-1
C₃₄H₄₆N₂O₇

Guidance literature:: C₁₉H₂₇NO₅; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 0.25h; Inert atmosphere;

C₁₅H₂₁NO₃*C₂HF₃O₂; In dichloromethane; at 20 ℃; for 8h; Inert atmosphere;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 111466-55-8
((2S,3S)-3-(2-(benzyloxy)ethyl)oxiran-2-yl)methanol

: 1543006-58-1
C₃₄H₄₆N₂O₇

Guidance literature:: Multi-step reaction with 16 steps

1.1: copper(l) iodide / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 1.5 h / -40 - 0 °C / Inert atmosphere

1.3: 0.5 h / 0 - 20 °C / Inert atmosphere

2.1: camphor-10-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 4 h / 20 °C / Inert atmosphere

4.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

5.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

6.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

7.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

8.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

9.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

10.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

11.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

11.2: 36 h / Inert atmosphere; Reflux

12.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

13.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

14.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

14.2: 1 h / -78 - 0 °C / Inert atmosphere

15.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

16.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / Inert atmosphere

16.2: 8 h / 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium tetrahydroborate; sodium periodate; sodium dihydrogenphosphate; copper(l) iodide; osmium(VIII) oxide; sodium azide; 2-methyl-but-2-ene; oxalyl dichloride; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; acetic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 1586791-90-3
C₁₈H₂₈O₅

: 1543006-58-1
C₃₄H₄₆N₂O₇

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

2.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

3.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

4.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

5.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

6.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

7.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

8.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

8.2: 36 h / Inert atmosphere; Reflux

9.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

11.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

11.2: 1 h / -78 - 0 °C / Inert atmosphere

12.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

13.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0.25 h / Inert atmosphere

13.2: 8 h / 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium tetrahydroborate; sodium periodate; sodium dihydrogenphosphate; sodium azide; 2-methyl-but-2-ene; oxalyl dichloride; tetrabutyl ammonium fluoride; water; benzotriazol-1-ol; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.12.078