(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II)

Base Information

• Chemical Name: (5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II)
• CAS No.: 445487-66-1
• Molecular Formula: C₄₄H₈F₂₀N₄Ni
• Molecular Weight: 1031.23
• Mol file: 445487-66-1.mol

Synonyms:(5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II)

Chemical Property of (5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II)

There total 10 articles about (5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

tetrakis(pentafluorophenyl)porphyrin (25440-14-6) + nickel(II) acetylacetonate → (5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II) (445487-66-1)

Guidance literature:

In toluene; for 96h; Reflux;

DOI:10.1039/c4cc05525j

Reference yield: 96.0%

tetrakis(pentafluorophenyl)porphyrin (25440-14-6) → (5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II) (445487-66-1)

Guidance literature:

With nickel chloride pentahydrate; In dimethyl sulfoxide; at 154 ℃; for 3h;

DOI:10.1016/j.tetlet.2014.01.049

Reference yield: 90.0%

5,10,15,20-tetrakis(pentafluorophenyl)porphyrin + nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) → (5,10,15,20-tetrakis(pentafluorophenyl)porphyrinato)nickel(II) (445487-66-1)

Guidance literature:

In N,N-dimethyl-formamide; acetonitrile; for 6h; Inert atmosphere; Reflux;

DOI:10.1039/c7sc02073b

upstream raw materials:

nickel(II) acetate tetrahydrate

nickel diacetate

tetrakis(pentafluorophenyl)porphyrin

Downstream raw materials:

Ni(C₂₀H₈N₄(C₆F₄O(CH₂)3NC₄H₄)(C₆F₅)3)

Ni(C₂₀H₈N₄(C₆F₄O(CH₂)3NC₄H₄)2(C₆F₅)2)

Ni(C₂₀H₈N₄(C₆F₄O(CH₂)3NC₄H₄)3(C₆F₅))

C₅₄H₁₆F₂₀N₈NiO₄