[(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(II)Fe(II)-Cl]B(C₆F₅)4

Base Information

• Chemical Name: [(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(II)Fe(II)-Cl]B(C₆F₅)4
• CAS No.: 825638-77-5
• Molecular Formula: C₂₄BF₂₀*C₆₃H₄₀ClF₆Fe₂N₈O
• Molecular Weight: 1865.24

Synonyms:[(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(II)Fe(II)-Cl]B(C₆F₅)4

Chemical Property of [(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(II)Fe(II)-Cl]B(C₆F₅)4

Chemical Property:

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Technology Process of [(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(II)Fe(II)-Cl]B(C₆F₅)4

There total 4 articles about [(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(II)Fe(II)-Cl]B(C₆F₅)4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

[(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine(2-))Fe(III)-O-Fe(III)-Cl]B(C6F5)4 (825648-79-1,849726-84-7) → [(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine(2-))Fe(II)Fe(II)-Cl]B(C6F5)4 (825638-77-5)

Guidance literature:

With sodium dithionite; In dichloromethane; water; (Ar); addn. of a soln. of iron complex in CH2Cl2 to aq. soln. of sodium dithionite, stirring for 35 min; evapn., recrystn. (THF/heptane, overnight, room temp.), filtration, drying in vac.;

DOI:10.1021/ja0458773

Reference yield:

FeClN(CH2C5H4N)2CH2C5H3NCH2OC6H4C20H8N4OFe(C6H3F2)3(1+)*B(C6F5)4(1-)=Fe2OClN(CH2C5H3N)3OC7H8C20H8N4(C6H3F2)3B(C6F5)4 (825648-79-1,849726-84-7) → [(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine(2-))Fe(II)Fe(II)-Cl]B(C6F5)4 (825638-77-5)

Guidance literature:

In tetrahydrofuran; Irradiation (UV/VIS); N2; UV-photolysis of THF-soln. of complex for 1 h; detected by spectra;

DOI:10.1021/ic0490932

Reference yield:

FeO2(C5H2N)4(C6H3F2)3C6H4OCH2C5H3NCH2N(CH2C5H4N)2FeCl(1+)*B(C6F5)4(1-)=FeO2C38H17N4F6C25H23ON4FeClB(C6F5)4 → [(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine(2-))Fe(II)Fe(II)-Cl]B(C6F5)4 (825638-77-5) + oxygen (80937-33-3)

Guidance literature:

In tetrahydrofuran; Irradiation (UV/VIS); UV irradn. of a soln. of iron complex in THF at 198 K; not isolated, detected by UV;

DOI:10.1021/ja045195f

upstream raw materials:

FeClN(CH₂C₅H₄N)2CH₂C₅H₃NCH₂OC₆H₄C₂₀H₈N₄OFe(C₆H₃F₂)3⁽¹⁺⁾*B(C₆F₅)4^(1-)=Fe₂OClN(CH₂C₅H₃N)3OC₇H₈C₂₀H₈N₄(C₆H₃F₂)3B(C₆F₅)4

FeClN(CH₂C₅H₄N)2CH₂C₅H₃NCH₂OC₆H₄C₂₀H₈N₄⁽¹⁸⁾OFe(C₆H₃F₂)3⁽¹⁺⁾*B(C₆F₅)4^(1-)=Fe₂OCl(CH₂C₅H₃N)3⁽¹⁸⁾OC₂₇H₁₆N₅(C₆H₃F₂)3B(C₆F₅)4

[(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(III)-O-Fe(III)-Cl]B(C₆F₅)4

Downstream raw materials:

[(5-ortho-O-[(N,N-bis(2-pyridylmethyl)-2-(6-methoxy)pyridinemethanamine)phenyl]-10,15,20-tris(2,6-difluorophenyl)porphine^(2-))Fe(III)-O-Fe(III)-Cl]B(C₆F₅)4

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