4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin

Base Information

Chemical Name:4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin
CAS No.:105379-08-6
Molecular Formula:C₂₇H₂₈Cl₂N₂
Molecular Weight:451.439
Hs Code.:

Synonyms:4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin

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Technology Process of 4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin

There total 4 articles about 4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 104-88-1
4-chlorobenzaldehyde

: 105378-77-6
1-<2-(4-Chlorphenylethyl)>-4-phenylpiperidin-4-yl-methanamin

: 105379-08-6
4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 3h; Heating;
DOI:10.1002/ardp.19863190606

Reference yield:

: 40481-13-8
4-phenyl-4-cyanopiperidine

: 105379-08-6
4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent

2: 75 percent / LiAlH₄ / tetrahydrofuran

3: 70 percent / p-toluenesulfonic acid / toluene / 3 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1002/ardp.19863190606

Reference yield:

: 105378-94-7
1-(4-Cyano-4-phenylpiperidin-1-yl)-2-(4-chlorphenyl)-1-ethanon

: 105379-08-6
4-Chlorphenyl-N-<1-<2-(4-chlorphenylethyl)>-4-phenylpiperidin-4-yl>-methanimin

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / LiAlH₄ / tetrahydrofuran

2: 70 percent / p-toluenesulfonic acid / toluene / 3 h / Heating

With lithium aluminium tetrahydride; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;
DOI:10.1002/ardp.19863190606