phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Base Information

Chemical Name:phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside
CAS No.:1030632-45-1
Molecular Formula:C₃₁H₅₆O₇Si₂
Molecular Weight:596.952
Hs Code.:

Synonyms:phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

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Technology Process of phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

There total 2 articles about phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1030632-42-8
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-(p-nitrobenzoyl)-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

: 1030632-45-1
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol800697k

Reference yield:

: 1030632-42-8
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-(p-nitrobenzoyl)-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

: 1030632-45-1
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

: C₃₁H₅₆O₇Si₂

Guidance literature:: With methanol; potassium carbonate;
DOI:10.1021/ol800697k

Reference yield: 95.0%

: 865484-73-7
tert-butyl ((2S,6S)-6-methyl-5-oxo-5,6-dihydro-2H-pyran-2-yl) carbonate

: 1030632-45-1
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

: 1030632-48-4
phenylmethyl 3-O-(tert-butyldimethylsilyl)-4-O-[3-O-[(2R,6S)-5,6-dihydro-6-methyl-5-oxo-2H-pyran-2-yl]-4-O-(tert-butyldimethylsilyl)-β-D-olivopyranosyl]-β-D-olivopyranoside

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; triphenylphosphine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol800697k