2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵-[1,3,5,2]triazaphosphinine

Base Information

• Chemical Name: 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵-[1,3,5,2]triazaphosphinine
• CAS No.: 65288-70-2
• Molecular Formula: C₃₀H₁₀F₃₄N₃O₄P
• Molecular Weight: 1153.35

Synonyms:2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵-[1,3,5,2]triazaphosphinine

Chemical Property of 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵-[1,3,5,2]triazaphosphinine

Chemical Property:

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Technology Process of 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵-[1,3,5,2]triazaphosphinine

There total 5 articles about 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ⁵-[1,3,5,2]triazaphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

(1Z,6Z)-2,2,4,4-Tetraphenyl-6,8-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-ethyl]-2λ5,4λ5-[1,3,5,7,2,4]tetrazadiphosphocine → 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5-[1,3,5,2]triazaphosphinine (65288-70-2) + Perfluoro-2,5-dimethyl-3,6-dioxanonanonitril (57697-79-7) + 1,1,1,2,2,3,3,5,6,6,8,9,9,9-Tetradecafluoro-4,7-dioxa-5-(trifluoromethyl)-nonane (3330-14-1) + hexaphenyl-cyclotriphosphazene (1110-78-7) + benzene (71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1)

Guidance literature:

With air; at 316 ℃; for 24h; Product distribution; various temp.; effect of oxigen;

DOI:10.1016/S0022-1139(00)82366-0

Reference yield: 11.0%

(1Z,6Z)-2,2,4,4-Tetraphenyl-6,8-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-ethyl]-2λ5,4λ5-[1,3,5,7,2,4]tetrazadiphosphocine → 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5-[1,3,5,2]triazaphosphinine (65288-70-2) + Perfluoro-2,5-dimethyl-3,6-dioxanonanonitril (57697-79-7) + 1,1,1,2,2,3,3,5,6,6,8,9,9,9-Tetradecafluoro-4,7-dioxa-5-(trifluoromethyl)-nonane (3330-14-1) + hexaphenyl-cyclotriphosphazene (1110-78-7)

Guidance literature:

at 316 ℃; for 24h;

DOI:10.1016/S0022-1139(00)82366-0

Reference yield:

2,3,3,3-Tetrafluoro-2-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-propionamidine + diphenyltrichlorophosphorane (1017-89-6) → 2,2,4,4-tetraphenyl-6-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5,4λ5-[1,3,5,2,4]triazadiphosphinine (70242-76-1) + 2,2-diphenyl-4,6-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropoxy-propoxy)-ethyl]-2λ5-[1,3,5,2]triazaphosphinine (65288-70-2) + (1Z,4Z)-2,2,6,6-Tetraphenyl-4,8-bis-[1,2,2,2-tetrafluoro-1-(1,1,2,3,3,3-hexafluoro-2-heptafluoropropyloxy-propoxy)-ethyl]-2λ5,6λ5-[1,3,5,7,2,6]tetrazadiphosphocine

Guidance literature:

Title compound not separated from byproducts; 1.) 108 - 114 deg C, 24 h, 2.) 123 - 132 deg C, 114 h;

DOI:10.1016/S0022-1139(00)82365-9

upstream raw materials:

diphenyltrichlorophosphorane

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