(R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester

Base Information

Chemical Name:(R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester
CAS No.:475983-37-0
Molecular Formula:C₁₉H₂₀F₅NO₄
Molecular Weight:421.364
Hs Code.:

Synonyms:(R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester

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Technology Process of (R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester

There total 1 articles about (R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 144085-23-4
N-tert-butoxycarbonyl-L-α-allylproline

: 475983-37-0
(R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 ℃;
DOI:10.1021/jo025999i

Reference yield: 54.0%

: 475983-37-0
(R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester

: 475983-39-2
(R)-1-(tert-butoxycarbonyl)-6-oxo-7-oxa-1-azaspiro[4.5]decane

Guidance literature:: (R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester; With 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; at 20 ℃; for 4h;

With sodium hydroxide; dihydrogen peroxide; In tetrahydrofuran; at 20 ℃; for 0.75h; Further stages.;
DOI:10.1021/jo025999i

Reference yield:

: 475983-37-0
(R)-N-(tert-butoxycarbonyl)-2-allylproline pentafluorophenyl ester

: 475983-65-4
(2R)-N-[(1S)-1-(benzyloxycarbonyl)-3-methylbutyl]-1-(tert-butoxycarbonyl)-2-(3-hydroxypropyl)pyrrolidine-2-carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: 9-BBN / tetrahydrofuran / 4 h / 20 °C

1.2: 54 percent / H₂O₂; 3N NaOH / tetrahydrofuran / 0.75 h / 20 °C

2.1: 50 percent / 2-hydroxypyridine / toluene / 72 h / Heating

With 2-hydroxypyridin; 9-borabicyclo[3.3.1]nonane dimer; In tetrahydrofuran; toluene;
DOI:10.1021/jo025999i