[(5-tBu-2-(Me2NCH2)C6H3)Ga(η6-C6H5)2Mo]2

Base Information

• Chemical Name: [(5-tBu-2-(Me2NCH2)C6H3)Ga(η6-C6H5)2Mo]2
• CAS No.: 1035458-31-1
• Molecular Formula: C₅₀H₆₀Ga₂Mo₂N₂
• Molecular Weight: 1020.37
• Mol file: 1035458-31-1.mol

Synonyms:[(5-tBu-2-(Me2NCH2)C6H3)Ga(η6-C6H5)2Mo]2

Chemical Property of [(5-tBu-2-(Me2NCH2)C6H3)Ga(η6-C6H5)2Mo]2

Chemical Property:

Purity/Quality:

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Technology Process of [(5-tBu-2-(Me2NCH2)C6H3)Ga(η6-C6H5)2Mo]2

There total 1 articles about [(5-tBu-2-(Me2NCH2)C6H3)Ga(η6-C6H5)2Mo]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

dilithiobis(benzene)molybdenum*N,N,N',N'-tetramethylethylenediamine + (5-tBu-2-(Me2NCH2)C6H3)GaCl2 (1035458-26-4) → bis(benzene)molybdenum (12129-68-9) + [(5-tBu-2-(Me2NCH2)C6H3)Ga(η6-C6H5)2Mo]2 (1035458-31-1)

Guidance literature:

In benzene; byproducts: LiCl*(CH3)2NCH2CH2N(CH3)2; (inert atm.); addn. of suspn. of molybdenum compd. in benzene to benzenesoln. of gallium compd. at 0°C, stirring for 1 h without cooling bath; evapn., extn. (toluene), filtration, cooling filtrate at -25°C, isolation of crystals, washing with benzene, drying in vac., elem. anal.;

DOI:10.1021/ic800336f

upstream raw materials:

(5-tBu-2-(Me₂NCH₂)C₆H₃)GaCl₂