3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane

Base Information

• Chemical Name: 3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane
• CAS No.: 921601-16-3
• Molecular Formula: C₅₂H₇₀N₄O₉
• Molecular Weight: 895.149
• Mol file: 921601-16-3.mol

Synonyms:3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane

Chemical Property of 3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane

There total 1 articles about 3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

3,3,7,7-tetra(hydroxymethyl)-5-oxanonane (23235-61-2) + 2-chloro-N-ethylacetanilide (39086-61-8) → 3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane (921601-16-3)

Guidance literature:

With sodium hydride; In tetrahydrofuran; for 6h; Heating;

DOI:10.1016/j.saa.2006.04.008

Reference yield:

3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane (921601-16-3) + europium(III) perchlorate hexahydrate → [Eu(3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane)](perchlorate)3

Guidance literature:

In ethyl acetate; addn. of soln. of europium compd. in ethyl acetate to soln. of oxanonanederiv. in ethyl acetate, stirring for 4 h; collecting precipitate, washing with ethyl acetate, drying in vac., elem. anal.;

DOI:10.1016/j.saa.2006.01.053

Reference yield:

3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane (921601-16-3) + europium(III) perchlorate hexahydrate → [Eu(3,3,7,7-tetra[N-ethyl-N-phenyl(acetamide)-2-oxymethyl]-5-oxanonane)](ClO4)3

Guidance literature:

In ethyl acetate; ethyl acetate soln. of Eu(ClO4)3*6H2O added dropwise to soln. of ligand in ethyl acetate, stirred for 4 h; ppt. collected, washed with ethyl acetate, dried in vac.; elem. anal.;

DOI:10.1016/j.saa.2006.04.008

upstream raw materials:

3,3,7,7-tetra(hydroxymethyl)-5-oxanonane

2-chloro-N-ethylacetanilide