C₂₅H₃₈O₆SSi

Base Information

Chemical Name:C₂₅H₃₈O₆SSi
CAS No.:1316846-40-8
Molecular Formula:C₂₅H₃₈O₆SSi
Molecular Weight:494.725
Hs Code.:

C<sub>25</sub>H<sub>38</sub>O<sub>6</sub>SSi

Synonyms:C₂₅H₃₈O₆SSi

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Chemical Property of C₂₅H₃₈O₆SSi

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Technology Process of C₂₅H₃₈O₆SSi

There total 7 articles about C₂₅H₃₈O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1316846-39-5
C₂₅H₃₆O₅SSi

: 1316846-40-8
C₂₅H₃₈O₆SSi

Guidance literature:: C₂₅H₃₆O₅SSi; With boron trifluoride diethyl etherate; In diethyl ether; dichloromethane; at -78 - 0 ℃; for 4h;

With sodium hydrogencarbonate; In diethyl ether; dichloromethane; water; at 0 - 20 ℃; for 1h;

Reference yield:

: C₁₄H₁₈O₄

: 1316846-40-8
C₂₅H₃₈O₆SSi

Guidance literature:: Multi-step reaction with 6 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 0.5 h / -40 °C

1.2: 1 h / 0 °C

2.1: zinc(II) chloride / tetrahydrofuran / 0.25 h / 20 °C

2.2: 2.17 h / -78 °C

2.3: -78 - 20 °C

3.1: N-Bromosuccinimide; water / toluene / 0.25 h / 20 °C

4.1: potassium carbonate / acetonitrile / 8.25 h / 0 - 20 °C

5.1: 1H-imidazole / dichloromethane / 1 h / 20 °C

6.1: boron trifluoride diethyl etherate / diethyl ether; dichloromethane / 4 h / -78 - 0 °C

6.2: 1 h / 0 - 20 °C

With 1H-imidazole; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; potassium carbonate; zinc(II) chloride; lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane; dichloromethane; toluene; acetonitrile;

Reference yield:

: C₁₉H₂₀O₄S

: 1316846-40-8
C₂₅H₃₈O₆SSi

Guidance literature:: Multi-step reaction with 5 steps

1.1: zinc(II) chloride / tetrahydrofuran / 0.25 h / 20 °C

1.2: 2.17 h / -78 °C

1.3: -78 - 20 °C

2.1: N-Bromosuccinimide; water / toluene / 0.25 h / 20 °C

3.1: potassium carbonate / acetonitrile / 8.25 h / 0 - 20 °C

4.1: 1H-imidazole / dichloromethane / 1 h / 20 °C

5.1: boron trifluoride diethyl etherate / diethyl ether; dichloromethane / 4 h / -78 - 0 °C

5.2: 1 h / 0 - 20 °C

With 1H-imidazole; N-Bromosuccinimide; boron trifluoride diethyl etherate; water; potassium carbonate; zinc(II) chloride; In tetrahydrofuran; diethyl ether; dichloromethane; toluene; acetonitrile;