3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone

Base Information

Chemical Name:3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone
CAS No.:1431372-54-1
Molecular Formula:C₁₄H₁₈O₂
Molecular Weight:218.296
Hs Code.:

Synonyms:3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone

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Technology Process of 3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone

There total 4 articles about 3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1431372-71-2
1-methoxy-2-[(E)-3-(2-methylallyloxy)prop-1-enyl]benzene

: 1431372-54-1
3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; In 1,2-dichloro-ethane; at 80 ℃; for 16h; chemoselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1021/ol400574s

Reference yield:

: 24393-54-2
ethyl 3-(2-methoxyphenyl)prop-2-enoate

: 1431372-54-1
3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone

Guidance literature:: Multi-step reaction with 3 steps

1.1: diisobutylaluminium hydride / dichloromethane; hexane / 2 h / -78 °C / Inert atmosphere

2.1: sodium hydride / paraffin oil; tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

3.1: 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate / 1,2-dichloro-ethane / 16 h / 80 °C / Inert atmosphere; Schlenk technique

With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; sodium hydride; diisobutylaluminium hydride; In tetrahydrofuran; hexane; dichloromethane; 1,2-dichloro-ethane; paraffin oil;
DOI:10.1021/ol400574s

Reference yield:

: 1504-61-6,13523-28-9,114568-19-3
(E)-3-(2-methoxyphenyl)prop-2-en-1-ol

: 1431372-54-1
3-(2-methoxyphenyl)-2,2-dimethylcyclopentanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / paraffin oil; tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate / 1,2-dichloro-ethane / 16 h / 80 °C / Inert atmosphere; Schlenk technique

With 1,1'-bis-(diphenylphosphino)ferrocene; bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; sodium hydride; In tetrahydrofuran; 1,2-dichloro-ethane; paraffin oil;
DOI:10.1021/ol400574s