ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate

Base Information

Chemical Name:ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate
CAS No.:1093863-68-3
Molecular Formula:C₂₃H₃₂O₂
Molecular Weight:340.506
Hs Code.:

Synonyms:ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate

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Chemical Property of ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate

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Technology Process of ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate

There total 1 articles about ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1093863-56-9
(+)-(4R)-2-iodo-1-methyl-4-(prop-1-en-2-yl)cyclohex-1-ene

: 252930-80-6
(2E,4E,6Z,8E)-9-Iodo-3,7-dimethyl-nona-2,4,6,8-tetraenoic acid ethyl ester

: 1093863-68-3
ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate

Guidance literature:: (+)-(4R)-2-iodo-1-methyl-4-(prop-1-en-2-yl)cyclohex-1-ene; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h;

With Trimethyl borate; In tetrahydrofuran; hexane; at 0 - 20 ℃;

(2E,4E,6Z,8E)-9-Iodo-3,7-dimethyl-nona-2,4,6,8-tetraenoic acid ethyl ester; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; TlOH; In tetrahydrofuran; hexane; water; at 25 ℃; for 0.5h;
DOI:10.1016/j.bmc.2008.09.069

Reference yield: 77.0%

: 1093863-68-3
ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate

: 1093863-51-4
(-)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoic acid

Guidance literature:: ethyl (+)-(2E,4E,6Z,8E)-3,7-dimethyl-9-[(5R)-2-methyl-5-(prop-1-en-2-yl)cyclohex-1-ene]nona-2,4,6,8-tetraenoate; With potassium hydroxide; water; In ethanol; for 0.5h; Reflux;

With hydrogenchloride; water; In ethanol;
DOI:10.1016/j.bmc.2008.09.069