(+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-⁽⁶⁾

Base Information

• Chemical Name: (+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-⁽⁶⁾
• CAS No.: 107420-43-9
• Molecular Formula: C₅₈H₄₇NO₇
• Molecular Weight: 870.014

Synonyms:(+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-⁽⁶⁾

Chemical Property of (+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-⁽⁶⁾

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Technology Process of (+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-⁽⁶⁾

There total 4 articles about (+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-⁽⁶⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-imin-(6) (107062-70-4) → (+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-(6) (107420-43-9)

Guidance literature:

With phosphoric acid; In 1,4-dioxane; Heating;

DOI:10.1021/ja00867a023

Reference yield:

2,2',3,3',4,4'-hexakis(benzyloxy)-1,1'-biphenyl-6,6'-dicarboxylic acid (97152-40-4) → (+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-(6) (107420-43-9)

Guidance literature:

Multi-step reaction with 4 steps

1: LiAlH₄

2: PBr₃

3: dimethylformamide

4: aq. H₃PO₄ / dioxane / Heating

With lithium aluminium tetrahydride; phosphoric acid; phosphorus tribromide; In 1,4-dioxane; N,N-dimethyl-formamide;

DOI:10.1021/ja00867a023

Reference yield:

(+/-)-4,4',5,5',6,6'-Hexakis-benzyloxy-2,2'-bis-brommethyl-biphenyl (149020-60-0) → (+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-on-(6) (107420-43-9)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide

2: aq. H₃PO₄ / dioxane / Heating

With phosphoric acid; In 1,4-dioxane; N,N-dimethyl-formamide;

DOI:10.1021/ja00867a023

upstream raw materials:

(+/-)-2'.3'.4'.1''.2''.3''-Hexakis-(benzyloxy)-5-cyan-1.2.3.4-dibenz-cycloheptadien-(1.3)-imin-⁽⁶⁾

2,2',3,3',4,4'-hexakis(benzyloxy)-1,1'-biphenyl-6,6'-dicarboxylic acid

(+/-)-4,4',5,5',6,6'-Hexakis-benzyloxy-2,2'-bis-hydroxymethyl-biphenyl

(+/-)-4,4',5,5',6,6'-Hexakis-benzyloxy-2,2'-bis-brommethyl-biphenyl

Downstream raw materials:

(+/-)-2'.3'.4'.1''.2''.3''-Hexakis--5-cyan-1.2.3.4-dibenz-cyclohepta-dien-(1.3)-ol-(6)

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