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C16H22O4

Base Information
  • Chemical Name:C16H22O4
  • CAS No.:1243260-48-1
  • Molecular Formula:C16H22O4
  • Molecular Weight:278.348
  • Hs Code.:
C<sub>16</sub>H<sub>22</sub>O<sub>4</sub>

Synonyms:C16H22O4

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Chemical Property of C16H22O4
Chemical Property:
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Technology Process of C16H22O4

There total 5 articles about C16H22O4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
C17H20O6; With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; formic acid; triethylamine; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;
With water; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ol101753y
Guidance literature:
Multi-step reaction with 3 steps
1: AD-mix-α; methanesulfonamide / water; tert-butyl alcohol / 0 °C
2: tetrahydrofuran / 20 °C
3: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; formic acid; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; formic acid; methanesulfonamide; AD-mix-α; triethylamine; triphenylphosphine; In tetrahydrofuran; water; tert-butyl alcohol; 1: Sharpless dihydroxylation;
DOI:10.1021/jo2019762
Guidance literature:
Multi-step reaction with 2 steps
1: tetrahydrofuran / 20 °C
2: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; formic acid; triethylamine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C
With tris(dibenzylideneacetone)dipalladium(0) chloroform complex; formic acid; triethylamine; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/jo2019762
upstream raw materials:

C17H20O6

C16H20O3

C16H22O5

ethyl (2E)-4-(diethoxyphosphoryl)crotonate

Downstream raw materials:

C23H28O5

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