5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole

Base Information

Chemical Name:5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole
CAS No.:1451058-68-6
Molecular Formula:C₂₄H₂₉BrN₄O
Molecular Weight:469.424
Hs Code.:

Synonyms:5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole

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Chemical Property of 5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole

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Technology Process of 5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole

There total 5 articles about 5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1451058-54-0
4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenol

: 589-15-1
1-bromomethyl-4-bromobenzene

: 1451058-68-6
5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole

Guidance literature:: With potassium carbonate; In butanone; for 12h; Reflux;
DOI:10.1039/c3tc30966e

Reference yield:

: 767-00-0
4-cyanophenol

: 1451058-68-6
5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium azide; ammonium chloride / N,N-dimethyl-formamide / 24 h / 120 °C

2.1: sodium hydroxide / water / 0.5 h / Cooling with ice

3.1: potassium carbonate / acetone / 48 h / Reflux

4.1: potassium hydroxide / water; methanol / 12 h / Reflux

4.2: pH 2 / Cooling with ice

5.1: potassium carbonate / butanone / 12 h / Reflux

With sodium azide; potassium carbonate; ammonium chloride; potassium hydroxide; sodium hydroxide; In methanol; water; N,N-dimethyl-formamide; acetone; butanone;
DOI:10.1039/c3tc30966e

Reference yield:

: 1451058-52-8
4-[2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazol-5-yl]phenyl acetate

: 1451058-68-6
5-[4-(4-bromobenzyloxy)phenyl]-2-((3S)-3,7-dimethyloct-6-enyl)-2H-tetrazole

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / water; methanol / 12 h / Reflux

1.2: pH 2 / Cooling with ice

2.1: potassium carbonate / butanone / 12 h / Reflux

With potassium carbonate; potassium hydroxide; In methanol; water; butanone;
DOI:10.1039/c3tc30966e